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A versatile UHV transport and measurement chamber for neutron reflectometry under UHV conditions

机译:用于中子的多功能UHV输送和测量室   特高压条件下的反射计

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摘要

We report on a versatile mini ultra-high vacuum (UHV) chamber which isdesigned to be used on the MAgnetic Reflectometer with high Incident Angle ofthe J\"ulich Centre for Neutron Science at Heinz Maier-Leibnitz Zentrum inGarching, Germany. Samples are prepared in the adjacent thin film laboratory bymolecular beam epitaxy and moved into the compact chamber for transfer withoutexposure to ambient air. The chamber is based on DN 40 CF flanges and equippedwith sapphire view ports, a small getter pump, and a wobble stick, which servesalso as sample holder. Here, we present polarized neutron reflectivitymeasurements which have been performed on Co thin films at room temperature inUHV and in ambient air in a magnetic field of 200 mT and in the Q-range of 0.18\AA$^{-1}$. The results confirm that the Co film is not contaminated during thepolarized neutron reflectivity measurement. Herewith it is demonstrated thatthe mini UHV transport chamber also works as a measurement chamber which opensnew possibilities for polarized neutron measurements under UHV conditions.
机译:我们报告了一个多功能的微型超高真空(UHV)室,该室设计用于德国格辛市Heinz Maier-Leibnitz Zentrum的J \“ ulich中子科学中心的具有高入射角的磁反射仪上。在相邻的薄膜实验室采用分子束外延技术,并移至紧凑的腔室中进行传输,而不会暴露于环境空气中,该腔室基于DN 40 CF法兰,并配有蓝宝石观察孔,小型吸气泵和摆动棒(也可作为样品)在这里,我们介绍极化中子反射率的测量,该测量是在室温下,在特高压和环境空气中,在200 mT的磁场中以及在0.18 \ AA $ ^ {-1} $的Q范围内对Co薄膜进行的。结果证实,在极化中子反射率测量中,Co膜没有被污染,从而证明了微型特高压输电室也可以作为测量室,从而打开了新的特高压条件下极化中子测量的可能性。

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